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KitAlysis High-Throughput Copper C-N Cross-Coupling Reaction Screening Kit-Pack of 2

ALDRICH/KITALYSIS-CUCN

Product Type: Chemical

Catalog Number PKG Qty. Price Quantity
45-KITALYSIS-CUCN-2PK 2 pk
$804.00
1/EA
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KitAlysis™ C-N High-Throughout Screening Kit: catalysts, stir bars, preweighed bases, substrate vials, and ampules
12 × 2 preweighed catalysts with stir bars and cap mat
Anhydrous, degassed solvents
Internal standard
Provided substrate bottles, preweighed bases, and stir bars
Complete KitAlysis™ Screening Platform (some components sold seperately)

 

reaction suitability core: palladium
  reaction type: Buchwald-Hartwig Cross Coupling Reaction
  reaction type: Heck Reaction
  reaction type: Hiyama Coupling
  reaction type: Negishi Coupling
  reaction type: Sonogashira Coupling
  reaction type: Stille Coupling
  reaction type: Suzuki-Miyaura Coupling
  reagent type: catalyst
reaction type: Cross Couplings
Application: Screening kit for Copper C-N Cross-Coupling Reactions. Step-by-step user guides and a downloadable experimental excel sheets are provided in the below hyperlinks.

Step-by-Step Guide for KitAlysis High-Throughput Copper C-N Cross-Coupling Reaction Screening Kit 

Downloadable experimental excel sheet 

Each kit contains 2 customizable screening sets that include the following components:
• 24 (6 x 4) pre-weighed ligands in glass vials loaded with stir bars, topped with cap mat
• Potassium phosphate: 4 pre-weighed vials with product labels and lids
• CuI (soluble source) in preweighed vial
• 4 degassed anhydrous solvents (dioxane, DMAc, toluene, and DMSO) in ampules
• 1 internal standard
• 2 KitAlysis 24-Well reaction block replacement films
• 8 stir bars for stock solutions
• Ampule cracker

Monitor reaction progress via TLC-MS by following this protocol 

Best when used with KitAlysis Benchtop Inertion Box  and 24-well Reaction Block  (sold separately).
Features and Benefits: • Designed and tested by synthetic chemists.
• Easily run 24-microscale reaction in parallel.
• Suggested conditions: 10 μmol reactions with 1 μmol catalyst (10 mol%) 0.1 M concentration, and 3 equiv. base.
• Customizable and downloadable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks.
Legal Information: KitAlysis is a trademark of Sigma-Aldrich Co. LLC
UNSPSC 12352200

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