KitAlysis™ High-Throughput Medium (5, 6, 7) Ring Closing Metathesis Reaction Screening Kit - Pack of 2
ALDRICH/KITALYSIS-RCM
Product Type: Equipment/Book
KitAlysis™ C-N High-Throughout Screening Kit: catalysts, stir bars, preweighed bases, substrate vials, and ampules
Anhydrous, degassed solvents
12 × 2 preweighed catalysts with stir bars and cap mat
Complete KitAlysis™ Screening Platform (some components sold seperately)
Provided substrate bottles, preweighed bases, and stir bars
Internal standard
| reaction suitability | core: palladium |
| reaction type: Buchwald-Hartwig Cross Coupling Reaction | |
| reaction type: Heck Reaction | |
| reaction type: Hiyama Coupling | |
| reaction type: Negishi Coupling | |
| reaction type: Sonogashira Coupling | |
| reaction type: Stille Coupling | |
| reaction type: Suzuki-Miyaura Coupling | |
| storage temp. | 2-8°C |
| Application: | Screening kit for ring closing metathesis. Step-by-step user guides and a downloadable experimental excel sheets are provided in the below hyperlinks. Step-by-Step Guide for Ring Closing Metathesis/Cross Metathesis Reaction Screening Kit  Downloadable experimental excel file Each kit contains 2 customizable screening sets that include the following components: • 6x4 pre-weighed catalysts in glass microvials loaded with stir bars and topped with cap mat. • 2 (2 mL) ampules each of of ClPh, PhMe, i-PrOAc, Me-THF, and TFA. • 1 KitAlysis 24-well reaction block replacement film. • 4 empty substrate stock solution reaction vials with stir bars. • 1 internal standard. Monitor reaction progress via TLC-MS by following this protocol Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately). |
| Features and Benefits: | • Designed and tested by synthetic chemists. • Easily run 24-microscale reaction in parallel. • 20 μmol reactions with 1 μmol catalyst (5 mol%), 0.2 M concentration, and optional TFA additive. • Customizable and downloadable excel template for quick calculations and easy incorporation into electronic laboratory notebooks. |
| Legal Information: | KitAlysis is a trademark of Sigma-Aldrich Co. LLC |
| Symbol |      GHS02,GHS05,GHS07,GHS08,GHS09 |
| Signal word | Danger |
| Hazard statements | H228 - H302 + H332 - H315 - H318 - H336 - H361d - H373 - H411 |
| Precautionary statements | P210 - P273 - P280 - P304 + P340 + P312 - P305 + P351 + P338 - P308 + P313 |
| RIDADR | UN 3316 9 |
| WGK Germany | WGK 3 |
| Supplemental Hazard Statements | EUH019 |
| Storage Temp. | 2-8°C |
| UNSPSC | 12161600 |
| Components | Grubbs Catalyst® M204, Umicore 3 µmol; Hoveyda-Grubbs Catalyst® M720, Umicore, 97% 3 µmol; Grubbs Catalyst® M102, Umicore, 97% 3 µmol; Grubbs Catalyst® M207, Umicore 3 µmol; Hoveyda-Grubbs Catalyst® M721, Umicore 3 µmol; Hoveyda-Grubbs Catalyst® M722, Umicore 3 µmol; Isopropyl acetate, anhydrous, ZerO2®, ≥99.6% 8 mL; 2-Methyltetrahydrofuran, anhydrous, contains 250 ppm BHT as stabilizer, ZerO2®, ≥99.0% 8 mL; Chlorobenzene, anhydrous, ZerO2®, 99.8% 8 mL; Toluene, anhydrous, ZerO2®, 99.8% 8 mL; Spinbar® magnetic stirring fleas, red, L 10 mm, diam. 3 mm 1 EA; SnapIT Ampule Opener, Regular, for 1-2ml, 5-10ml, 10-15ml ampoules 1 EA |