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Dichloromethane

SIAL/439223 - suitable for HPLC, ≥99.9%, contains 40-150 ppm amylene as stabilizer

Synonym: Methylene chloride

CAS Number: 75-09-2
Empirical Formula (Hill Notation): CH2Cl2
Molecular Weight: 84.93
EC Number: 200-838-9
MDL Number: MFCD00000881
Linear Formula: CH2Cl2
Product Type: Chemical

Catalog Number PKG Qty. Price Quantity
45-439223-4L 4 L
$235.00
1/EA
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45-439223-4X4L 4 L
$777.00
4/EA
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45-439223-VB200LP1SB 4 L
No Price  

 

λ H2O reference
assay ≥99.9%
autoignition temp. 1223 °F
bp 39.8-40 °C (lit.)
color APHA: ≤10
  clear
contains 40-150 ppm amylene as stabilizer
density 1.325 g/mL at 25 °C (lit.)
evapn. residue <0.0003%
expl. lim. 22 %
form liquid
impurities Free halogens, passes test
  ≤0.0003 meq/g Titr. acid
  ≤0.02% water
InChI 1S/CH2Cl2/c2-1-3/h1H2
InChI key YMWUJEATGCHHMB-UHFFFAOYSA-N
mp −95 °C (lit.)
Quality Level 100 
refractive index n20/D 1.424 (lit.)
SMILES string ClCCl
suitability passes test for HPLC
technique(s) HPLC: suitable
UV absorption λ: 235 nm Amax: 1.00
  λ: 240 nm Amax: 0.20
  λ: 250 nm Amax: 0.05
  λ: 260 nm Amax: 0.02
  λ: 340-400 nm Amax: 0.01
vapor density 2.9 (vs air)
vapor pressure 24.45 psi ( 55 °C)
  6.83 psi ( 20 °C)
Application: Dichloromethane (Methylene chloride) may be used in the following processes:
• To compose ultrasonic baths for cleaning and protection of aluminum coating over atactic-PMMA (poly(methyl methacrylate)) for dielectric studies.
• Preparation of AMBF3 (ammoniomethyltrifluoroborate)-conjugated biomolecules.
• Sample preparation for GC-MS (Gas Chromatography-Mass Spectrometry) analysis.
• Preparation of ammonium acetate solvent mixture in combination with isopropanol, acetonitrile and water for mass spectral analysis of neutral lipids.
• Quantification of glutathione (GSH) and glutathione disulfide (GSSG) in biological samples by HPLC and spectrophotometry.
• As an extractant for 2,2-dithioethyl-4-(2′-pyridyl)-4-butyro-γ-lactone.
Application: Meets ACS specifications
General description: Dichloromethane (DCM) is a chlorinated organic solvent with a wide range of industrial applications. It has C2v symmetry, low boiling point, high density and is immiscible in water. Degradation of DCM by various methods has been reported. Ultrasonic absorption studies of liquid DCM shows strong relaxation effect. A study reports the dielectric characteristics of DCM over a wide frequency range. DCM is susceptible to degradation with time, which can be suppressed by adding amylene as a stabilizer.
Packaging: 4, 4×4 L in PVC-coated bottle
Preparation Note: Product filtered through a 0.2 μm filter
Purity ≥99.9%
bp 39.8-40 °C (lit.)
mp −95 °C (lit.)
Density 1.325 g/mL at 25 °C (lit.)
Refractive Index n20/D 1.424 (lit.)
UNSPSC 12190000

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