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Multi-Layer Silica Gel SPE Tube

SUPELCO/52732-U - configured for US EPA Method 8290, PTFE frit, glass hardware, volume 6 mL, pk of 30

Synonym: Glass Silica Gel SPE (for EPA 8290), 6 mL

Product Type: Equipment/Book

Catalog Number PKG Qty. Price Quantity
45-52732-U 30 ea
$522.00
1/EA
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application(s) food and beverages
compatibility configured for US EPA Method 8290
composition bed A, 0.1 g (silica)
  bed B, 0.2 g (basic silica (2% KOH coated))
  bed C, 0.4 g (acidic silica (22% H2SO4 coated))
  bed D, 0.2 g (silica)
material glass hardware
  PTFE frit
packaging pk of 30
Quality Level 100 
technique(s) solid phase extraction (SPE): suitable
volume 6 mL
General description: Developed specifically for use with US EPA Method 8290 - "Polychlorinated Dibenzodioxins (PCDDs) AND Polychlorinated Dibenzofurans (PCDFs) by High-Resolution Gas Chromatography/High-Resolution Mass Spectrometry (HRGC/HRMS)"

The sample clean-up employed in EPA Method 8290 requires a series of hand-packed glass chromatography steps involving: 1) a mult-layer silica gel class column, 2) a sodium sulfate/alumina glass column, and 3) a multi-layer celite 545-activated carbon glass column.

Cat. No. 52732-U can be used in place of the required multi-layer silica gel glass column, and Cat. No. 52733-U can be used in place of the required multi-layer celite 545-activated carbon glass column.

Note that the bed weights packed into these SPE tubes are smaller than what is described in EPA Method 8290. Therefore, to use these SPE tubes, sample volumes need to be scaled down accordingly.
UNSPSC 41115712

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